Infrared surface spectroscopy and surface optical reflectance for operando catalyst surface characterization
Using a new sample environment, the two operando surface diagnostic techniques two-dimensional surface optical reflection (2D-SOR) and polarization-modulated infrared reflection–absorption spectroscopy (PM-IRRAS) have been combined with mass spectrometry (MS) to characterize a catalytic reaction. With both techniques integrated in a custom-built setup, we can correlate molecular information of the